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<http://digilib.unila.ac.id/id/eprint/14775> <http://purl.org/dc/terms/title> "Transesterifikasi Minyak Sawit dengan\r\nMetanol dan Katalis Heterogen Berbasis\r\nSilika Sekam Padi (TiO2/SiO2)"^^<http://www.w3.org/2001/XMLSchema#string> .
<http://digilib.unila.ac.id/id/eprint/14775> <http://purl.org/ontology/bibo/abstract> "Abstrak\r\n\r\nPenelitian ini mempelajari reaksi transesterifikasi minyak kelapa sawit dengan\r\nmetanol dan katalis heterogen berbasis silika sekam padi, yakni TiO2/SiO2.\r\nPreparasi katalis dilakukan dengan metode sol-gel yang dipadukan dengan metode\r\nultasonifikasi menggunakan sol silika yang dihasilkan dari sekam padi dan larutan\r\nTiCl3, untuk menghasilkan katalis dengan kadar dopan 5% terhadap berat silika\r\nsekam padi. Selanjutnya katalis dikalsinasi pada suhu 700°C dengan kenaikan\r\nsuhu 3 oC/menit dan ditahan selama 3 jam pada suhu puncak. Uji katalis dalam\r\nreaksi transesterifikasi minyak sawit dilakukan untuk mempelajari pengaruh\r\nvariabel kinetis yakni nisbah katalis 5 dan 10%, perbandingan mol minyak sawit\r\nterhadap metanol 1:4, 1:6, dan 1:8, dan waktu reaksi 15, 30, dan 45 menit. Hasil\r\npenelitian menunjukkan kondisi optimum adalah penggunaan katalis Ti sebesar\r\n10% terhadap berat minyak sawit, dengan perbandingan mol minyak kelapa sawit\r\ndan metanol 1:4, pada suhu 60oC selama 30 menit dengan persen konversi sebesar\r\n90,91%. Berdasarkan analisis parameter biodiesel diperoleh produk\r\ntransesterifikasi yang memenuhi standar SNI 04-7182-2006 yakni viskositas 4,49\r\nmm2/s, cetane number 98,5, dan massa jenis 0,87 g/mL. Berdasarkan analisis\r\nmenggunakan GC-MS dapat dipastikan bahwa produk yang dihasilkan dari reaksi\r\ntransesterifikasi minyak kelapa sawit adalah metil ester asam lemak (biodiesel).\r\nKomposisi terbesar dalam biodiesel yang dihasilkan adalah metil palmitat, yakni\r\nsebesar 97,70% sebagai kandungan utama minyak sawit. Hasil ini menunjukkan\r\nbelum semua asam lemak mampu diubah menjadi metil esternya sehingga\r\ndiperlukan penelitian lebih lanjut.\r\nKata kunci: minyak sawit, biodiesel, katalis heterogen\r\n\r\n\r\n\r\n\r\n\r\n\r\n\r\n\r\nAbstract\r\n\r\nThis research studied the transesterification of palm oil with methanol and\r\nheterogeneous catalysts based on rice husk silica, ie TiO2/SiO2. Preparation of the\r\ncatalyst was conduted by sol-gel method combined with ultasonification method\r\nusing silica sol produced from rice husk and TiCl3 solution, to produce a catalyst\r\nwith 5% dopant levels. Furthermore, the catalyst was calcined at a temperature of\r\n700 oC with a temperature rise of 3oC/minute and held for 3 h at peak temperature.\r\nThe catalysts was tested for transesterification of palm oil to study the influence\r\nof kinetic variables including catalyst ratio, mole ratio of palm oil to methanol,\r\nand reaction time. The results revealed that the optimum condition is the use of\r\n10% catalyst, mole ratio of palm oil and methanol 1:4, at a temperature of 60 ° C\r\nfor 30 minutes with the percent conversion rate of 90.91%. The biodiesel\r\nproduced meet, the SNI 04-7182-2006 in terms of viscosity (4.49 mm2 / s), cetana\r\nnumber (98.5), and density (0.87 g / mL). Analysis using GC-MS can indicated\r\nthat the main component in the biodiesel is methyl palmitate, which amounted to\r\n97.70%.\r\nKey word: palm oil. biodiesel, heterogeneous catalysts"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/14775/69/medium.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "medium.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/14775/70/small.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "small.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/id/document/1256916> <http://purl.org/dc/terms/hasPart> <http://digilib.unila.ac.id/14775/71/lightbox.jpg> .
<http://digilib.unila.ac.id/14775/71/lightbox.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "lightbox.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/14775/76/preview.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "preview.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/14775/77/medium.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "medium.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/id/document/1256923> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1252094> .
<http://digilib.unila.ac.id/id/document/1256923> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1252094> .
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<http://digilib.unila.ac.id/id/document/1256923> <http://purl.org/dc/terms/hasPart> <http://digilib.unila.ac.id/14775/78/small.jpg> .
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