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<http://digilib.unila.ac.id/id/eprint/23123> <http://purl.org/dc/terms/title> "PREPARASI DAN KARAKTERISASI NANOKATALIS Ni0,6 Fe2Co0,4O4 UNTUK REAKSI HIDROGENASI KATALITIK CO2"^^<http://www.w3.org/2001/XMLSchema#string> .
<http://digilib.unila.ac.id/id/eprint/23123> <http://purl.org/ontology/bibo/abstract> "Pada penelitian ini telah dibuat nanokatalis Ni0,6Fe2Co0,4O4 dengan metode sol- gel dan freezedry menggunakan pektin, serta dilakukan uji aktivitas katalitiknya terhadap reaksi konversi (CO2/H2) menjadi alkohol pada suhu 200 – 400°C. Hasil karakterisasi katalis setelah kalsinasi 600 °C menunjukan terbentuknya 3 fasa kristalin yaitu Fe2NiO4 (25,3%), Fe3O4 (51,5%), dan CoFe2O4 (23,2%). Hasil analisis ukuran XRD menggunakan persamaan Scherrer dan analisis menggunakan SEM menunjukan ukuran katalis pada rentang 118 - 220 nm. Hasil analisis ukuran distribusi partikel menggunakan PSA menghasilkan katalis berskala nanometer pada rentang 0 - 2 %. Hasil uji aktivitas katalitik menunjukkan bahwa katalis Ni0,6Fe2Co0,4O4 aktif dan memiliki selektifitas yang tinggi. Analisis menggunakan kromatografi gas menunjukkan bahwa katalis Ni0,6Fe2Co0,4O4 pada suhu kalsinasi 600°C dengan suhu reaksi 200 °C paling aktif terhadap konversi CO2/H2 menghasilkan propanol yaitu 53134,83 ppm.\r\nKata kunci ; nanokatalis, pektin, PSA, Scherrer, solgel-freezedry, SEM\r\n\r\n\r\n\r\nABSTRAK BAHASA INGGRIS\r\n\r\nIn this study, nano catalyst Ni0,6Fe2Co0,4O4 has been prepared by sol gel – freeze dry method using pectin as an emulsifying agent, and then the sample was subjected to calcination treatment and subsequently characterized using the techniques of X-ray diffraction (XRD), Rietveld and Scherrer Methods, FTIR, PSA and SEM analysis. Its catalytic activity was tested for CO2/H2 conversion to alcohol at a temperature of 200 - 400°C. The results of XRD characterization indicated that Ni0,6Fe2Co0,4O4 calcined at 600°C materials consist of three crystalline phases which are Fe2NiO4(25.3%), Fe3O4 (51.5%), and CoFe2O4 (23.2%). The results of size analysis using both Scherrer method and SEM show that the size of the catalyst is in the range of 11,8 – 22,0 nm. Then, particle size analyzer (PSA) proved that particle size distribution is in the range of 0-2%. Catalytic activity tests showed that Ni0,6Fe2Co0,4O4 nanocatalysts are active. Product analysis using gas chromatography indicates that the Ni0,6Fe2Co0,4O4 nanocatalyst calcined at 600°C is the most active for conversion of CO2/H2 at a reaction temperature of 200 °C and propanol yield is 53134.83 ppm.\r\nKeywords; nano catalysts, pectin, , sol gel – freeze dry, alcohol"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/id/document/1670978> <http://eprints.org/relation/islightboxThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670978> <http://eprints.org/ontology/hasFile> <http://digilib.unila.ac.id/23123/11/lightbox.jpg> .
<http://digilib.unila.ac.id/id/document/1670978> <http://purl.org/dc/terms/hasPart> <http://digilib.unila.ac.id/23123/11/lightbox.jpg> .
<http://digilib.unila.ac.id/23123/11/lightbox.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "lightbox.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
<http://digilib.unila.ac.id/id/eprint/23123> <http://eprints.org/ontology/hasDocument> <http://digilib.unila.ac.id/id/document/1670979> .
<http://digilib.unila.ac.id/id/document/1670979> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://eprints.org/ontology/Document> .
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<http://digilib.unila.ac.id/id/document/1670979> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670979> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670979> <http://eprints.org/relation/ispreviewThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670979> <http://eprints.org/ontology/hasFile> <http://digilib.unila.ac.id/23123/12/preview.jpg> .
<http://digilib.unila.ac.id/id/document/1670979> <http://purl.org/dc/terms/hasPart> <http://digilib.unila.ac.id/23123/12/preview.jpg> .
<http://digilib.unila.ac.id/23123/12/preview.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "preview.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
<http://digilib.unila.ac.id/id/eprint/23123> <http://eprints.org/ontology/hasDocument> <http://digilib.unila.ac.id/id/document/1670980> .
<http://digilib.unila.ac.id/id/document/1670980> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://eprints.org/ontology/Document> .
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<http://digilib.unila.ac.id/id/document/1670980> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670980> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670980> <http://eprints.org/relation/ismediumThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670980> <http://eprints.org/ontology/hasFile> <http://digilib.unila.ac.id/23123/13/medium.jpg> .
<http://digilib.unila.ac.id/id/document/1670980> <http://purl.org/dc/terms/hasPart> <http://digilib.unila.ac.id/23123/13/medium.jpg> .
<http://digilib.unila.ac.id/23123/13/medium.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "medium.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/id/document/1670981> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://eprints.org/ontology/Document> .
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<http://digilib.unila.ac.id/id/document/1670981> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670981> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
<http://digilib.unila.ac.id/id/document/1670981> <http://eprints.org/relation/issmallThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670951> .
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<http://digilib.unila.ac.id/id/document/1670981> <http://purl.org/dc/terms/hasPart> <http://digilib.unila.ac.id/23123/14/small.jpg> .
<http://digilib.unila.ac.id/23123/14/small.jpg> <http://www.w3.org/2000/01/rdf-schema#label> "small.jpg"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/id/document/1670982> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://eprints.org/ontology/Document> .
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<http://digilib.unila.ac.id/id/document/1670982> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670982> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670982> <http://eprints.org/relation/islightboxThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
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<http://digilib.unila.ac.id/id/document/1670983> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://eprints.org/ontology/Document> .
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<http://digilib.unila.ac.id/id/document/1670983> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670983> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670983> <http://eprints.org/relation/ispreviewThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/eprint/23123> <http://eprints.org/ontology/hasDocument> <http://digilib.unila.ac.id/id/document/1670984> .
<http://digilib.unila.ac.id/id/document/1670984> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://eprints.org/ontology/Document> .
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<http://digilib.unila.ac.id/id/document/1670984> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670984> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670984> <http://eprints.org/relation/ismediumThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/eprint/23123> <http://eprints.org/ontology/hasDocument> <http://digilib.unila.ac.id/id/document/1670985> .
<http://digilib.unila.ac.id/id/document/1670985> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://eprints.org/ontology/Document> .
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<http://digilib.unila.ac.id/id/document/1670985> <http://eprints.org/relation/isVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670985> <http://eprints.org/relation/isVolatileVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/document/1670985> <http://eprints.org/relation/issmallThumbnailVersionOf> <http://digilib.unila.ac.id/id/document/1670952> .
<http://digilib.unila.ac.id/id/eprint/23123> <http://www.w3.org/2000/01/rdf-schema#seeAlso> <http://digilib.unila.ac.id/23123/> .
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<http://digilib.unila.ac.id/23123/> <http://purl.org/dc/elements/1.1/format> "text/html" .
<http://digilib.unila.ac.id/23123/> <http://xmlns.com/foaf/0.1/primaryTopic> <http://digilib.unila.ac.id/id/eprint/23123> .
<http://digilib.unila.ac.id/id/subject/Q> <http://www.w3.org/1999/02/22-rdf-syntax-ns#type> <http://www.w3.org/2004/02/skos/core#Concept> .
<http://digilib.unila.ac.id/id/subject/Q> <http://www.w3.org/2004/02/skos/core#prefLabel> " "@en .
<http://digilib.unila.ac.id/id/eprint/23123> <http://purl.org/dc/terms/subject> <http://digilib.unila.ac.id/id/subject/Q> .