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<http://digilib.unila.ac.id/id/eprint/24640> <http://purl.org/dc/terms/title> "ANALISIS STRUKTUR DAN LUAS PERMUKAAN SPESIFIK ZEOLIT\r\nBERBASIS SILIKA SEKAM PADI AKIBAT VARIASI SUHU KALSINASI\r\n150 oC, 250 oC, DAN 350oC"^^<http://www.w3.org/2001/XMLSchema#string> .
<http://digilib.unila.ac.id/id/eprint/24640> <http://purl.org/ontology/bibo/abstract> "ABSTRAK\r\n\r\nPenelitian tentang “Analisis Struktur dan Luas Permukaan Spesifik Zeolit\r\nBerbasis Silika Sekam Padi Akibat Variasi Suhu Kalsinasi 150oC, 250oC, dan\r\n350oC. Penelitian ini bertujuan untuk mempelajari pengaruh suhu kalsinasi\r\nterhadap perubahan fasa dan luas permukaan spesifiknya. Sintesis zeolit dibuat\r\ndari bahan silika sekam padi, NaOH, dan alumina dengan metode sol gel dan\r\nperlakuan kalsinasi suhu 150oC, 250oC, dan 350oC. Sampel zeolit dikarakterisasi\r\ndengan difraksi sinar-X (XRD) dan Surface Area Analyzer (SAA). Dari hasil\r\nXRD diperoleh fasa yang terbentuk dan ukuran kristalit menggunakan persamaan\r\nScheerer. Pada suhu 150oC, fasa yang terbentuk gibbsite dengan ukuran kristalit\r\n61,21 nm. Sedangkan pada suhu 250oC terdapat fasa gibbsite, bohmite, dan quartz\r\ndengan ukuran kristalit berturut-turut adalah 58,71 nm; 180,06 nm; dan 80,35 nm.\r\nPada suhu 350oC fasa gibbsite telah berubah sepenuhnya menjadi bohmite dengan\r\nukuran kristalit 112,37 nm dan adanya quartz dengan ukuran kristalit 30,14 nm.\r\nSemakin kecil ukuran kristalit, maka luas permukaan spesifik zeolit akan semakin\r\nbesar. Dari hasil analisis SAA luas permukaan spesifik akibat suhu kalsinasi\r\n150oC, 250oC, dan 350oC masing-masing adalah 106,900 m2/g; 90,650 m2/g; dan\r\n241,970 m2/g. Dari hasil penelitian diketahui ukuran kristalit fasa pada suhu\r\n350oC memiliki nilai paling kecil, sehingga diperoleh luas permukaan spesifik\r\npaling besar.\r\nKata kunci: Fasa, kalsinasi, luas permukaan spesifik, ukuran kristalit, dan zeolit.\r\n\r\nABSTRACT\r\n\r\nThe synthesis and analysis zeolite based silica rice husk was conducted by a\r\nvariety temperature of calcination at 150oC, 250oC, and 350oC. This research has\r\npurpose to study influence temperature of calcination to the phase and specific\r\nsurface area zeolite. Zeolite was synthesized from silica rice husk, NaOH, and\r\nalumina by sol gel method, and thermally treated 150oC, 250oC, and 350oC, then\r\ncharacterized using X-ray Diffraction (XRD) and Surface Area Analyzer (SAA).\r\nXRD characterization was obtained phase and crystalline size using Scheerer\r\nequation. At temperature 150oC results gibbsite phase with crystalline size 61,21\r\nnm. At temperature 250oC results gibbsite, bohmite, and quartz with crystalline\r\nsize successively 58,71 nm; 180,06 nm; and 80,35 nm. At temperature 350oC\r\nresults gibbsite phase had transformed to bohmite phase with crystalline size\r\n112,37 nm, then quartz phase with crystalline size 30,14 nm. Small crystalline\r\nsize produce high specific surface area. The smaller crystalline size, the higher\r\nspecific surface area. SAA results specific surface area at temperature 150oC,\r\n250oC, and 350oC respectively are106,900 m2/g; 90,650 m2/g; and 241,970 m2/g.\r\nBased on the result, it can be concluded that the smallest crystalline size and the\r\nlargest specific surface area in temperature 350oC.\r\nKeywords: Crystalline size, calcinations, phase, specific surface area, and zeolite.\r\n\r\n"^^<http://www.w3.org/2001/XMLSchema#string> .
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<http://digilib.unila.ac.id/id/subject/QC> <http://www.w3.org/2004/02/skos/core#prefLabel> "QC Physics"@en .
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