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primary topic: http://digilib.unila.ac.id/id/eprint/911

http://digilib.unila.ac.id/id/eprint/911
type: Article
title: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210)
abstract: Pada penelitian ini, telah dilakukan sintesis senyawa dibutiltimah(IV) di-4- nitrobenzoat, difeniltimah(IV) di-4-nitrobenzoat dan trifeniltimah(IV) 4- nitrobenzoat melalui dua tahap. Tahap pertama yaitu pembentukan senyawa antara organotimah(IV) hidroksida atau oksida dari organotimah(IV) klorida dan NaOH, kemudian direaksikan dengan asam 4-nitrobenzoat untuk menghasilkan senyawa akhir. Dari hasil sintesis diperoleh produk berupa padatan berwarna putih dengan rendemen 87,27; 88,33, dan 86,53 % untuk masing-masing senyawa dibutiltimah(IV) di-4-nitrobenzoat, difeniltimah(IV) di-4-nitrobebzoat dan trifeniltimah(IV) 4-nitrobenzoat dengan waktu refluks optimum 4 jam. Senyawa awal dan senyawa hasil sintesis dikarakterisasi dengan menggunakan spektrofotometer IR dan UV untuk melihat gugus fungsi dan λmax yang terdapat pada senyawa. Selain itu dilakukan juga analisis unsur dengan menggunakan microelemental analyzer terhadap senyawa hasil sintesis. Berdasarkan data hasil mikroanalisis, senyawa yang diperoleh telah murni karena perbedaan data yang diperoleh dengan perhitungan secara teori masih berkisar 1-5%. Uji pendahuluan aktivitas antikanker terhadap sel leukemia L-1210 diperoleh nilai IC50 untuk senyawa dibutiltimah(IV) di-4-nitrobenzoat, difeniltimah(IV) di-4-nitrobenzoat dan trifeniltimah(IV) 4-nitrobenzoat beturut-turut adalah 18,8; 8,8; dan 2,27 μg/mL. (In this study, it was performed the synthesis of dibutyltin(IV) di-4-nitrobenzoate, diphenyltin(IV) di-4-nitrobenzoate and triphenyltin(IV) 4-nitrobenzoate compounds through two-step reactions. The first step was the formation of the organotin(IV) hydroxide or oxide by reacting the organotin(IV) chloride and NaOH, then reacting the organotin(IV) hydroxide or oxide with 4-nitrobenzoic acid to produce the final compound. The results of synthesis were in the form of white solid with percent yield for dibutyltin(IV) di-4-nitrobenzoate, diphenyltin(IV) di-4-nitrobenzoate and triphenyltin(IV) 4-nitrobenzoate of 87.27; 88.33…
date: 2013-09-23
status: published
author list: authors
type: EPrint
type: OtherEPrint
is part of: repository
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Fakultas MIPA
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Sherly Nurimani Arpan
type: Person
given name: Sherly Nurimani
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http://digilib.unila.ac.id/id/document/58186
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58187
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http://digilib.unila.ac.id/id/document/58188
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http://digilib.unila.ac.id/id/document/58189
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http://digilib.unila.ac.id/id/document/58190
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http://digilib.unila.ac.id/id/document/58192
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http://digilib.unila.ac.id/id/document/58198
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http://digilib.unila.ac.id/id/document/58199
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http://digilib.unila.ac.id/id/document/58201
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http://digilib.unila.ac.id/id/document/58202
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http://digilib.unila.ac.id/id/document/58203
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http://digilib.unila.ac.id/id/document/58217
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58218
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58219
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58220
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58221
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58222
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58223
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58224
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58225
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58226
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58227
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58228
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/id/document/58229
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label: SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210) (Other)
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http://digilib.unila.ac.id/911/
title: HTML Summary of #911 SINTESIS DAN KARAKTERISASI SERTA UJI PENDAHULUAN AKTIVITAS ANTIKANKER BEBERAPA SENYAWA ORGANOTIMAH(IV) 4-NITROBENZOAT TERHADAP SEL LEUKEMIA L-1210 (SYNTHESIS, CHARACTERIZATION AND PRELIMINARY ANTICANCER ACTIVITY TEST OF SOME ORGANOTIN(IV) 4-NITROBENZOATES AGAINST LEUKEMIA CELLS L-1210)
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primary topic: http://digilib.unila.ac.id/id/eprint/911

Q Science (General)
type: Concept

QD Chemistry
type: Concept